Why PVD coating lines suffer from pumping-speed fluctuation

Throughput and film consistency on a coating line are decided to a large extent in the pumping stage. The same chamber with the same load takes six minutes to reach the handover pressure on the morning shift and eight and a half on the afternoon shift. Nothing was changed and no alarm was raised, yet the cycle will not hold. In most cases the pump is not broken: the effective pumping speed has dropped in the middle of the pressure range.

A PVD vacuum system is sensitive to pumping-speed fluctuation because three things depend on it at once: cycle time (one extra minute of roughing is one extra minute per batch), base pressure (if the chamber is not low enough before the process starts, adhesion and uniformity drift), and process pressure (sputtering runs at a working pressure in the 10⁻³ to 10⁻² mbar range, held by a throttle valve and a mass flow controller; if the backing side is weak, no amount of throttling recovers it). Sizing therefore needs four steps: duty checklist, roughing calculation, process-gas calculation, pump set configuration.

1. Build the duty checklist first

Coating lines all look like “pump to high vacuum” until the details are written down. Fill in the eight items below before looking at any model; leave two blank and the configuration is a guess.

ItemWhat to recordWhy it drives pumping speed
Chamber volumeNet empty volume including fixtures and workPump-down time scales with volume
Allowed roughing timeSeconds from atmosphere to handover pressureSets the minimum effective pumping speed
Handover pressurePressure at which the backing pump hands overCommonly in the 5-20 mbar range
Process working pressurePressure and gas type held during sputteringDefines the process-gas load
Process gas flowsccm of argon or other working gasConverts directly into a throughput figure
Pumped mediaDust, moisture, solvent vapour, target volatilesDecides filtration, condensation and gas ballast
Diversity factorHow many chambers share one pump setShared pumps split the available speed at peaks
PipingDistance, bore, bends and valves from pump room to chamberThe largest hidden discount on effective speed

2. Roughing: calculate the pump-down time

In the rough vacuum range, use the isothermal approximation t = (V / S) × ln(p₁ / p₂), where V is chamber volume, S the effective pumping speed and p₁, p₂ the start and target pressures. From 1013 mbar to 10 mbar, ln(1013/10) is about 4.62.

Chamber volumePumpRated speedIdeal timeAt 70% effective speed
0.5 m³DPL-V0155150 m³/h55 s79 s
1.0 m³DPL-V0202200 m³/h83 s119 s
2.0 m³DPL-V0302300 m³/h111 s158 s
2.5 m³DPL-V300B240 m³/h actual173 s247 s
3.0 m³DPL-V630B640 m³/h actual78 s111 s

The second time column is the one to quote for cycle planning. The 70% factor is a coarse allowance for piping and valves; small bore, long runs and many bends push it lower still. This is not measurement error but the most frequently ignored loss in a vacuum system: the speed measured at the chamber and the speed measured after fifteen metres of pipe can differ by half.

Two further effects flatten the curve: outgassing from walls and fixtures, and leakage at seals and flanges. Neither scales linearly with pressure, and both become visible as the target pressure is approached. This is also why gas ballast is normally opened during roughing: it admits dry air and lowers the partial pressure of condensable components so that water vapour leaves with the mixture instead of condensing in the oil. The cost is a higher ultimate pressure, so the ballast is closed again before pulling down to the handover point.

3. Process stage: gas load sets the floor for the backing pump

Roughing moves air; sputtering moves process gas. The relation is Q = p × S. One sccm is roughly 1.27 × 10⁻² mbar·L/s, so 200 sccm of argon is about 2.54 mbar·L/s. Spread over different backing pressures:

Backing pressureSpeed required for 200 sccm
0.5 mbar18.3 m³/h
0.3 mbar30.5 m³/h
0.1 mbar91.4 m³/h
0.05 mbar182.9 m³/h

The conclusion is blunt: the lower the backing pressure, the harder the backing pump works. The same 200 sccm needs about 20 m³/h at 0.5 mbar and more than 180 m³/h at 0.05 mbar. Backing pump size cannot be discussed apart from the pressure at which it runs, which is why one model is sufficient on one line and marginal on the next.

4. Roots stage: nameplate speed only holds at high inlet pressure

Above roughly 1.5 m³, or when the cycle is tight, a mechanical pump alone is not enough and a Roots set is used. The usual mistake is treating Roots speed as a constant.

The LC series covers 250, 500, 1200, 2600 and 4200 m³/h at 50 Hz, with motor ratings of 2.2, 2.2, 4.0, 7.5 and 11 kW and inlet flanges from ISO63 to ISO250. Those figures hold when inlet pressure is high enough. As inlet pressure falls, the volume a Roots pump can move falls with it, and actual speed increasingly depends on what the backing pump still delivers at the same point. Typical pairings are 2V80 (74 m³/h, 3 kW) with LC250, and 2V275 (255 m³/h, 7.5 kW) with LC2600, for coating chamber roughing and large chamber evacuation.

Roots rotors do not touch and seal on clearance, so excessive differential pressure overloads the motor. On WSU2000, maximum permissible differential pressure is 50 mbar with 2050 m³/h, 7.5 kW and DN160 ISO-K flanges; that 50 mbar is the interlock boundary. Start the backing pump first, bring the inlet to the set pressure, then start the Roots stage, and limit differential pressure with a bypass or overflow valve rather than letting the backing pump absorb it.

5. Configuration by chamber volume

Chamber volumeHandoverPumpMotorUltimate (ballast closed)Upgrade
0.3-0.6 m³10 mbarDPL-V0155 (150 m³/h)4.0 kW0.3 mbarLC250 for tight cycles
0.6-1.2 m³10 mbarDPL-V0202 (200 m³/h)5.5 kW0.1 mbarLC500
1.2-2.0 m³10 mbarDPL-V0302 (300 m³/h)7.5 kW0.5 mbarLC500 / LC1200
2.0-3.0 m³, tight footprint10 mbarDPL-V300B (280 nominal / 240 actual m³/h)5.5 kW≤0.08 mbarLC500
Above 3.0 m³ or fast cycle10 mbarDPL-V630B (700 nominal / 640 actual m³/h)15 kW≤0.08 mbarLC1200 or larger
Base pressure below 10⁻² mbar—DPL-2V80 / 2V275 with Roots3 / 7.5 kW4×10⁻⁴ / 5×10⁻⁴ mbarRecheck backing speed at the backing pressure

For V300B and V630B both nominal and actual speeds are listed: calculate cycle time on the actual figure. Nominal speed is geometric displacement, actual speed is measured, and the 8-9% difference is exactly what decides the seconds in the pump-down table.

6. Common pitfalls

  1. Comparing nameplate speed without fixing the working pressure. Two pumps 20% apart on the plate can differ twofold in actual speed at 0.05 mbar, because the curve is falling in that range.
  2. Piping sized to the pump flange instead of to the flow. A G2" inlet does not mean a G2" line: bends, bellows and valves each have to be checked. Piping loss is the only factor that lengthens the cycle without changing the pump.
  3. Sizing a shared pump set for a single chamber. Shared sets need the peak sum times the diversity factor; they save hardware but pass pressure excursions to every chamber.
  4. Leaving gas ballast open all day. It suppresses condensables at the cost of ultimate pressure and higher oil temperature. Close it before pulling down to the handover pressure.
  5. Ignoring oil condition. Pumping speed on an oil-sealed pump follows oil state: emulsified oil, low level or high temperature all reduce speed, and this is the most common physical reason a line is fast in the morning and slow in the afternoon.
  6. Copying 50 Hz data to 60 Hz supplies. Speed and motor ratings change with frequency. Some models are not suitable for 60 Hz regions; confirm before ordering for export projects.

Frequently asked questions

1 m³ chamber from atmosphere to 10 mbar, is DPL-V0202 enough?
The ideal time at 200 m³/h is 83 seconds, about 119 seconds at 70% effective speed. Acceptable when the process allows two minutes or more; for a 90-second cycle add an LC500 Roots stage and recheck the piping bore.
Why is the same pump fast in the morning and slow in the afternoon?
Check oil temperature and oil condition first, then the pressure drop across the inlet filter, then piping and valves. Only after those three are cleared should the pump itself be suspected.
Does a coating line always need a Roots pump?
It depends on volume and cycle. Below 0.6 m³ with a relaxed cycle, a single DPL-V0155 or DPL-V0202 handles roughing. Above 1.2 m³, or within 90 seconds, an LC250 or LC500 set is normally used, with the backing pump rechecked at its backing pressure.
How do I size the backing pump for 200 sccm of process gas?
Fix the backing pressure first. 200 sccm is about 2.54 mbar·L/s, requiring 30.5 m³/h at 0.3 mbar, 91.4 m³/h at 0.1 mbar and 182.9 m³/h at 0.05 mbar. Without a defined backing pressure there is no single answer.
When should gas ballast be opened and closed?
Open it during roughing when condensable components are present so they leave with the mixture instead of entering the oil; close it before pulling to the handover pressure. Leaving it open lowers ultimate pressure and raises oil temperature, and pumping speed changes with it.

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